Home | Contact Us | FAQ | Search & Site Map | Link to Us
Sign In | Join | Other 45 Sites in Network
Home
Discussion Groups
Biology
BiologyBotanyMicrobiologyEntomologyEvolutionPaleontology
Chemistry
General ChemistryAnalytical ChemistryElectrochemistryOrganic Synthesis
Earth Science
GeologyMineralogyOceanographyMeteorologyEarthquakes
Physics
General PhysicsResearchRelativityParticle PhysicsElectromagnetismFusionOpticsAcousticsNew Theories

Natural Science Forum / Chemistry / Organic Synthesis / June 2005


Tip: Looking for answers? Try searching our database.

dry PhONa and PhSNa

Thread view: 
Enable EMail Alerts  Start New Thread
Thread rating: 
Alex - 06 Jun 2005 11:17 GMT
Hello,

Could anyone suggest a good synthetic procedure for water free PhONa
and PhSNa?

Commercial samples do contain water.

Thanks!

Alex.
Reply to this Message
Namast? - 21 Jun 2005 10:02 GMT
Take the commercial samples, and then:

Sodium phenoxide: M 116.1. Washed with Et2O, then heated under vacuum
to 200? to
remove any free phenol.

I suposse that  sodium thiophenoxide and phenoxide could be dryed on
the Abderhalden pistol without any problem.

Bye.
Reply to this Message
 
Sign In
Join
My Latest Posts
My Monitored Threads
My Blog
My Photo Gallery
My Profile
My Homepage
Start New Thread
Enable EMail Alerts
Rate this Thread



©2009 Advenet LLC   Privacy Policy - Terms of Use
This website includes both content owned or controlled by Advenet as well as content owned or controlled by third parties.